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The catalysts show similar catalytic efficiency as the homogeneous catalyst in the model cyclopropanation between ethyl diazoacetate EDA and styrene. For ugtmann of material from all other RSC journals and books: DR-UV-vis and XPS demonstrate that the oxidation state and the Rh—Rh single bond in the dirhodium node are maintained during the ligand substitution process.

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The individual lamellae of the dirhodium-bdc frameworks are stacked as parallel sheets, which are randomly oriented or slightly ordered. Previous Article Next Article.

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Residual trifluoroacetate species are investigated by quantitative 19 F MAS NMR which further reflects the configuration of trifluoroacetate in the obtained Rh 2 -bdc Tfand defects in the structure. In all cases the Ref. The stability and gutmamn of the catalysts are verified by TG-DTA measurements and leaching tests. For reproduction of material from PCCP: You do not have JavaScript enabled.

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Catalytically active dirhodium sheet-like coordination polymers are synthesized from their precursors via ligand exchange. Heterogeneous self-supported dirhodium II catalysts with high catalytic efficiency in cyclopropanation — a structural study J.

Heterogeneous self-supported dirhodium II catalysts with high catalytic efficiency in cyclopropanation — a structural study. Fetching data from CrossRef. Aany Sofia Lilly Thankamony.